Aldehyde content of dialdehyde cellulose determined via nitrate analysis

نویسندگان

چکیده

Dialdehyde cellulose was synthesized via the heterogeneous periodate oxidation of microcrystalline in an aqueous solution. The aldehyde content dialdehyde determined nitrate analysis based on a two-step sequential approach. approach first employed hydroxylamine to react with groups and produce oxime Schiff’s replacement reaction. Then, were oxidized persulfate nitrate. concentration analyzed two highly sensitive methods, i.e., ion chromatography ultraviolet light absorption. approximately one-fifth theoretical value. resulting found primarily distributed over surface layers. A solubility parameter calculation suggested that increase caused detachment dissolution chains consequently led determination relatively low content.

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ژورنال

عنوان ژورنال: Bioresources

سال: 2022

ISSN: ['1930-2126']

DOI: https://doi.org/10.15376/biores.17.2.2457-2469